A Bijective Answer to a Question of Zvonkin by Ehrenborg R.

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By Ehrenborg R.

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The deposition of the precursor films was performed in a vacuum system equipped with a partly self-designed DC magnetron using a composit MgB2-Mg target. [106,107] The production step of ex-situ annealing was performed in a special designed experimental setup, where the precursor films and pure Mg powder are placed into a self sealing reactor, which consists of a Nb container and a Nb plunger both installed hermetically inside an evacuated quartz cylinder. The quartz tube is pumped down to 10-6 mbar.

The basic principle of these instruments is, almost like in mechanical profilometry, having a scanning tip which is moved line by line over a surface. The positioning technique which is used for tip movement and tip approach is piezoelectric technology. Modern piezoelectric elements[110] allow precise controlled movement of the tip on the sub Å scale. In case of scanning tunnelling microscopy (STM) the atomically sharp tip is held in constant distance from the surface. Typical distances are between 5 Å and 50 Å.

1: The influence of annealing time on the Tc , resistance broadening ∆Tc and R300/R40 for MgB2 films with a thickness of 1 µm prepared at annealing temperature of 850 ºC. 2: The influence of annealing temperature on the Tc , resistance broadening ∆Tc and R300/R40 for MgB2 films with a thickness of 1 µm prepared with an annealing period of 60 min. 2. Obviously, the optimal temperature regime for annealing MgB2 films is of about 850 °C and the optimum time for annealing is about 60 min. The films were grown on single crystal substrates of r-cut Al2O3 (1102) as well as of Al2O3 (100), MgO (100), and (1280 rot) LiNbO3 with a trigonal crystal structure.

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